主管：中华人民共和国司法部
主办：司法鉴定科学研究院
ISSN 1671-2072  CN 31-1863/N
Chinese Journal of Forensic Sciences

Chinese Journal of Forensic Sciences ›› 2011 ›› Issue (6): 23-25.

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Determination of Mercury in Human Hair by Inductively Coupled Plasma Mass Spectrometry

ZHANG Dan1,2,MA Dong2, ZHUO Xian-yi2   

  1. 1. Department of Forensic Medicine, Medical College of Soochow University, Suzhou 215123, China; 2. Shanghai Key laboratory of Forensic Medicine, Institute of Forensic Science, Ministry of Justice, Shanghai 200063, China
  • Received:2011-09-11 Published:2011-11-15 Online:2022-07-29

微波消解ICP-MS法测定人发中的汞

张 丹1，2，马 栋2，卓先义2   

  1. 1.苏州大学 医学部法医学系，江苏 苏州 215123；
    2.司法部司法鉴定科学技术研究所 上海市法医学重点实验室，上海 200063
  • 通讯作者: 卓先义（1957-），男，研究员，硕士研究生导师，主要从事毒物化学研究。
  • 作者简介:张丹（1985-），女，硕士研究生，主要从事毒物化学研究。E-mail: Zhang.Peonia@gmail.com

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Abstract: Objective To establish an inductively coupled plasma mass spectrometry(ICP-MS) method for the determination of mercury in human hair. Methods Samples were digested with microwave digestion instrument. ICP-MS was applied to determine the mercury in human hair, with 115In as an internal standard. Results The limits of detection was 0.0032 μg/g. Human hair certified reference materials (GBW09101b,GBW07601) were analyzed and excellent agreement with the certified value was obtained for mercury. Conclusion The method is rapid, effective, sensitive, accurate and suitable for the determination of mercury in human hair.

Key words: mercury, hair, inductively coupled plasma mass spectrometry, microwave digestion

摘要： 目的 建立人发中汞的电感耦合等离子体质谱分析方法。方法 采用微波消解法处理样品，以铟（115In）作内标，用电感耦合等离子体质谱分析人发中的汞含量。结果 方法检出限为0.0032 μg/g，准确度通过测定人发标准物质GBW07601、GBW09101b进行验证，检测结果与标准参考值相符。结论 该方法快捷、高效，灵敏度、准确度高，适用于人发中汞含量的检测。

关键词:  , 汞, 毛发, 电感耦合等离子体质谱法, 微波消解

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